CQU7037 – NMR APPLIED TO INORGANIC SYSTEMS

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LEVEL: Master and Doctorate

CREDITS: 6

MAIN TOPICS:

Physical bases of Nuclear Magnetic Resonance. Chemical shift and spin-spin coupling. Longitudinal and transverse relaxation. Fourier transform NMR pulse sequences. Multinuclear NMR. 2D-NMR. Experimental aspects and instrumentation. Selected experiments.

RECOMMENDED LITERATURE:

IGGO, J. A. NMR Spectroscopy in Inorganic Chemistry. Oxford: Oxford University Press, 2000.

CLARIDGE, T. D. W. High-Resolution NMR Techniques in Organic Chemistry. 2nd ed. Tetrahedron Organic Chemistry Series, v. 27. Amsterdam: Elsevier Science, 2008.

GÜNTHER, H. NMR Spectroscopy: basic principles, concepts, and applications in chemistry. 3rd ed. Chichester: John Wiley & Sons, 2013.

FRIEBOLIN, H. Basic One- and Two-Dimensional NMR Spectroscopy. 5th ed. Heidelberg: WileyVCH, 2011.

KEELER, J. Understanding NMR Spectroscopy. 2nd ed. New York: John Wiley & Sons, 2010.

NATURE PUBLISHING GROUP. Milestones in Spin. Trabesinger, A.; Wright, A. (Editors). http://www.nature.com/milestones/milespin/index.html. Assessed on 16/06/2017. L

EVITT, M. H. Spin Dynamics: basics of Nuclear Magnetic Resonance. 2nd ed. Chichester: John Wiley & Sons, 2008.

DEROME, A. E. Modern NMR Techniques for Chemical Research. Tetrahedron Organic Chemistry Series, v. 6. Series Editors: J. E. Baldwin and P. D. Magnus. Oxford: Pergamon, 1997.

DRAGO, R. S. Physical Methods for Chemists. 2nd ed. Philadelphia: Saunders College and Harcourt Brace Publishers, 1992. p. 500-518.

KOHLER, F. H. Paramagnetic Complexes in Solution: the NMR approach. eMagRes, 2011. DOI: DOI: 10.1002/9780470034590.emrstm1229.

BERTINI, I.; LUCHINAT, C. NMR of Paramagnetic Substances. Edited by A. B. P. Lever. Coord. Chem. Rev. v. 150, 1996. 296p.